File:Synthesis of Boc anhydride.png
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[edit]DescriptionSynthesis of Boc anhydride.png |
English: Synthesis of di-tert-butyl dicarbonate (Boc anhydride) by Dean Stanley Tarbell et al. in 1977. This file was made with ChemBioDraw Ultra 14. The digital object identifier of the reference is https://dx.doi.org/10.15227/orgsyn.057.0045. This image is intended to replace the original one (File:BOC_anhydride_synthesis.png) made by V8rik. Tarbell et al. started with alcohol-free potassium tert-butoxide instead of tert-butyl alcohol because alcohol-free base was more soluble in tetrahydrofuran and this made the forming of the tricarbonate successful. The typo of the solvent used (C6C6) has been fixed to C6H6. THF = tetrahydrofuran, cat = catalytic, rt = room temperature. |
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Author | Georginho |
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current | 19:19, 27 March 2016 | ![]() | 1,614 × 724 (21 KB) | Georginho (talk | contribs) | User created page with UploadWizard |
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