File:Synthesis Industrial Route 3.png

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Synthesis Industrial Route 3

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Deutsch: Nachdem [8] gebildet wurde muss für den folgenden Schritt der SnAr das zweite Edukt gebildet werden. Hierbei erfolgte ein Optimierungsschritt durch zusätzliche Chlorierung von [9], was für eine geringere Elektronendichte des Rings und somit eine starke Beschleunigung der Umsetzung sorgt. Dies wird in einer Zweischrittsynthese bewerkstelligt. Zunächst wird 6-Aminouracil [19] mit Chloracetaldehyd unter Aldoladdition und folgender Cyclisierung durch Aldolkondensation umgesetzt. Das entstandene Diol [20] wird durch Deoxychlorierung mit Phosphorylchlorid zum Dichlorid [21] umgesetzt.
Date
Source Own work
Author Kdalk04

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current19:42, 17 July 2023Thumbnail for version as of 19:42, 17 July 20231,052 × 163 (7 KB)Kdalk04 (talk | contribs)Uploaded own work with UploadWizard

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