File:Image from page 244 of "Practical methods of organic chemistry" (1901) (14584942120).jpg
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[edit]DescriptionImage from page 244 of "Practical methods of organic chemistry" (1901) (14584942120).jpg |
Identifier: practicalmethods00gatt Title: Practical methods of organic chemistry Year: 1901 (1900s) Authors: Gattemann, Ludwig. [from old catalog] Subjects: Publisher: [n.p.] Contributing Library: The Library of Congress Digitizing Sponsor: The Library of Congress
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Text Appearing After Image: FlG. 68. denser), pure benzene, boiling at 8i°, is obtained. Yield, about5 grammes. Monosubstituted hydrazines of the type of phenyl hydrazine maybe obtained according to the method of V. Meyer and Lecco,1 byreducing the diazo-compounds with stannous chloride and hydrochloricacid: 2 H. :CGH5.NH.NH2, HC1 Phenyl hydrazine hydrochloride The reaction is always conducted as above: The amine is diazotisedin a strong hydrochloric acid solution, and then a solution of stannouschloride in strong hydrochloric acid is added to it. Since the hydro-chlorides of the hydrazines are difficultly soluble in concentratedhydrochloric acid, these separate out directly on the addition of the 1 B. 16, 2976.Q 226 SPECIAL PART stannous chloride, and can easily be obtained pure by filtration, asabove. The reduction of the diazo-compounds to hydrazines may be ac-complished by the method of Emil Fischer1 which led to the dis-covery of this class of compounds, and also by another method. Ifneutral sodium sulphit
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Source | Image from page 244 of "Practical methods of organic chemistry" (1901) |
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